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HERO ID
1039274
Reference Type
Journal Article
Title
Continuous biodiesel production in a fixed bed reactor packed with anion-exchange resin as heterogeneous catalyst
Author(s)
Ren, Y; He, B; Yan, F; Wang, H; Cheng, Y; Lin, L; Feng, Y; Li, J
Year
2012
Is Peer Reviewed?
Yes
Journal
Bioresource Technology
ISSN:
0960-8524
EISSN:
1873-2976
Publisher
ELSEVIER SCI LTD
Location
OXFORD
Volume
113
Page Numbers
19-22
Language
English
PMID
22138595
DOI
10.1016/j.biortech.2011.10.103
Web of Science Id
WOS:000304223300005
Abstract
A continuous biodiesel production from the transesterification of soybean oil with methanol was investigated in a fixed bed reactor packed with D261 anion-exchange resin as a heterogeneous catalyst. The conversion to biodiesel achieved 95.2% within a residence time 56min under the conditions: reaction temperature of 323.15K, n-hexane/soybean oil weight rate of 0.5, methanol/soybean oil molar ratio of 9:1 and feed flow rate of 1.2ml/min. The resin can be regenerated in-situ and restored to the original activity to achieve continuous production after the resin deactivation. The product obtained was mainly composed of methyl esters. No glycerol in the product was detected due to the resin adsorbing glycerol in the fixed bed, which solved the issue of glycerol separation from biodiesel. It is believed that the fixed bed reactor with D261 has a potential commercial application in the transesterification of triglyceride.
Keywords
D261 anion-exchange resin; Biodiesel; Continuous transesterification; Fixed bed reactor; Heterogeneous catalyst
Tags
IRIS
•
Methanol (Non-Cancer)
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