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Citation
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HERO ID
1465047
Reference Type
Journal Article
Title
Extraction of Phthalate Esters in Environmental Water Samples Using Layered-Carbon Magnetic Hybrid Material as Adsorbent Followed by Their Determination with HPLC
Author(s)
Wang, W; Wu, Q; Zang, X; Wang, C; Wang, Zhi
Year
2012
Is Peer Reviewed?
Yes
Journal
Bulletin of the Korean Chemical Society
ISSN:
0253-2964
EISSN:
1229-5949
Publisher
WILEY-V C H VERLAG GMBH
Location
WEINHEIM
Volume
33
Issue
10
Page Numbers
3311-3316
Language
English
DOI
10.5012/bkcs.2012.33.10.3311
Web of Science Id
WOS:000310659900027
Abstract
In this paper, a layered-carbon-Fe3O4 (LC-Fe3O4) hybrid material was synthesized through a facile one-pot solvothermal method and used as the adsorbent for the preconcentration of some phthalate esters (dimethyl phthalate, diethyl phthalate, diallyl phthalate, diisobutyl phthalate and benzyl butyl phthalate) in water samples. The effects of the adsorbent dosage, extraction time, the solution pH and salinity on the adsorption of the phthalate esters (PAEs) were investigated. The magnetic nanocomposite adsorbent could remove and enrich the PAEs from water samples efficiently. After the adsorption, the analytes were desorbed and then determined by high performance liquid chromatography-ultraviolet detection. Under the optimum conditions, the enrichment factors of the method for the analytes were in the range from 161 to 180. A linear response with peak area as the quantification signal was observed in the concentration range from 0.5 to 100 ng mL(-1). The limits of detection (S/N = 3) of the method were between 0.08 and 0.1 ng mL(-1). The method was suitable for the determination of trace phthalate esters in environmental water samples.
Keywords
Adsorption; Determination; High performance liquid chromatography; Magnetic layered-carbon nanocomposite; Phthalate esters
Tags
IRIS
•
BBP (Butyl benzyl phthalate)
Literature Search
LitSearch Dec 2012
WOS
Excluded: No Primary Data on Health Effects
Measurement methods
•
Diethyl phthalate (DEP)
Database searches
Jan 2020 update
Web of Science
New for this project
Excluded: No Primary Data on Health Effects
Measurement methods
•
Diisobutyl Phthalate (DIBP) Final
Database Searches
March 2014 Database Search
Web of Science
September 2014 update
Web of Science
June 2015 Update
Web of Science
December 2015 Update
Web of Science
January 2017 Update
July 2017 Update
No Primary Data on Toxic Effects
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