Synthesis and Crystal Structure of 3-(3,4-Dimethylbenzylidene)-1,5-dioxaspiro[5.5]undecane-2,4-dione
Zeng, W
| HERO ID | 3830025 |
|---|---|
| In Press | No |
| Year | 2011 |
| Title | Synthesis and Crystal Structure of 3-(3,4-Dimethylbenzylidene)-1,5-dioxaspiro[5.5]undecane-2,4-dione |
| Authors | Zeng, W |
| Journal | Asian Journal of Chemistry |
| Volume | 23 |
| Issue | 9 |
| Page Numbers | 4145-4147 |
| Abstract | A new spiro compound 3-(3,4-dimethylbenzylidene)-1,5-dioxaspiro[5.5]undecane-2,4-dione was prepared by 1,5-dioxaspiro[5.5]undecane-2,4-dione with 3,4-dimethylbenzaldehyde in ethanol and its crystal structure was determined by X-ray crystallographic techniques. It crystallizes in monoclinic, space group Cc with a = 27.437(6) angstrom, b = 11.471(2) angstrom, c = 21.196(4) angstrom, beta = 109.85(3)degrees, C(18)H(20)O(4), Mr = 300.34, V = 6275(2) angstrom(3), Z = 16, Dc = 1.271 g/cm(3), F(000) = 2556, mu = 0.089 mm(-1). The 1,3-dioxane ring is in a distorted envelope conformation while cyclohexane ring assumes a highly symmetric chair conformation. |
| Wosid | WOS:000293193700085 |
| Url | https://www.scopus.com/inward/record.uri?eid=2-s2.0-80053345640&partnerID=40&md5=1a940269117aa881af019e6cd8c77c37 |
| Is Certified Translation | No |
| Dupe Override | No |
| Comments | Scopus URL: https://www.scopus.com/inward/record.uri?eid=2-s2.0-80053345640&partnerID=40&md5=1a940269117aa881af019e6cd8c77c37 |
| Is Public | Yes |
| Language Text | English |
| Keyword | Synthesis; Crystal structure; 1,5-Dioxaspiro[5.5]undecane-2,4-dione; Spiro compounds |