Synthesis of dibenzo[b,f][1,4]oxazepin-11(10H)-ones from 2-nitrobenzoic acids

Samet, AV; Kislyi, KA; Marshalkin, VN; Semenov, VV; ,

HERO ID

7686424

Reference Type

Journal Article

Year

2006

HERO ID 7686424
In Press No
Year 2006
Title Synthesis of dibenzo[b,f][1,4]oxazepin-11(10H)-ones from 2-nitrobenzoic acids
Authors Samet, AV; Kislyi, KA; Marshalkin, VN; Semenov, VV; ,
Journal Russian Chemical Bulletin
Page Numbers 549-553
Abstract Base-catalyzed intramolecular nucleophilic substitution for the 2-nitro group in 2-hydroxyanilides of 2-nitrobenzoic acids gave dibenzo[b,f][1,4]oxazepin-11(10H)-ones. In particular, 3 -nitrodibenzo[b,f][1,4] oxazepin-11 (10H)-one was obtained from N-(2-hydroxyphenyl)2,4-dinitrobenzamide. The nitro group in the product could also be replaced under the action of O- and S-nucleophiles.
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