Trace organic compounds in rain. 1. Sampler design and analysis by adsorption/thermal desorption (ATD)

Pankow, JF; Isabelle, LM; Asher, WE

HERO ID

32854

Reference Type

Journal Article

Year

1984

Language

English

HERO ID 32854
In Press No
Year 1984
Title Trace organic compounds in rain. 1. Sampler design and analysis by adsorption/thermal desorption (ATD)
Authors Pankow, JF; Isabelle, LM; Asher, WE
Journal Environmental Science & Technology
Volume 18
Issue 5
Page Numbers 310-318
Abstract The design and use of a rain sampler with a 0.89 m2 collection surface area were described. The sampler was controlled electronically, provided for the in situ filtration of the sample and carried out the preconcentration of nonpolar organic compounds by means of cartridges of the sorbent Tenax-GC. The possibility existed for including cartridges of ion-exchanging resin in the sampling train to provide for the preconcentration of organic acids. Analytical results were obtained for 27 compounds by fused silica capillary column gas chromatography with detection by mass spectrometry for 4 rain events sampled 12 km southwest of Portland, OR (USA), at the Oregon Graduate Center (OGC), and for 5 rain events sampled in Southeast Portland. Mean dissolved rain concentrations for alpha-BHC, naphthalene, acenaphthylene, fluorene and phenanthrene were 5.9, 11, 4.7, 3.2 and 24 ng/l, respectively, at OGC. The mean values for the Portland events were 47, 72, 55, 43 and 140 ng/l, respectively. Since dissolved concentrations were measured, the data were also used in conjunction with available Henry's law constants to estimate the concurrent, local atmospheric levels (H) of these compounds at these sites. Many of the H values of interest were available only near 298? K. The further understanding of the wet deposition of toxic organic compounds will be facilitated by the direct study of wet deposition and by the determination of the temperature dependence of the H values of environmentally interesting compounds.
Doi 10.1021/es00123a005
Wosid WOS:A1984SN91400010
Is Certified Translation No
Dupe Override No
Comments Scopus URL: https://www.scopus.com/inward/record.uri?eid=2-s2.0-0021550483&doi=10.1021%2fes00123a005&partnerID=40&md5=6a0259eb41a2ee1c528bb079c25e9124
Is Public Yes
Language Text English
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