Effect of the form of the quaternary ammonium ion on the ion-pair phase separation phenomenon with perfluorooctanoic acid

Yokohashi, G; Igarashi, S

HERO ID

3860752

Reference Type

Journal Article

Year

1997

Language

English

PMID

9056352

HERO ID 3860752
In Press No
Year 1997
Title Effect of the form of the quaternary ammonium ion on the ion-pair phase separation phenomenon with perfluorooctanoic acid
Authors Yokohashi, G; Igarashi, S
Journal Journal of Colloid and Interface Science
Volume 185
Issue 1
Page Numbers 278-280
Abstract The effect of the form of 10 types of quaternary ammonium ions (Q(+))for the phase separation phenomenon, which accompanies a charge neutralization with perfluorooctanoate ion (PFOA(-)) and Q(+), was studied, The separated phase using the spherical form of Q(+) (i.e., [4 . 4 . 4 . 4], [3 . 3 . 5 . 5], [3 . 3 . 3 . 7], and [2 . 2 . 6 . 6], where the numbers in square brackets represent the carbon numbers of four kinds of straight alkyl chains which were directly bonded to the nitrogen atom) was in the liquid state, On the other hand, the separated phase using the rod form ([2 . 2 . 2 . 10] and [1 . 1 . 1 . 13]) was in the solid state. The volume, specific gravity, and water content of the liquid-separated phase using [3 . 3 . 5 . 5] were 116 mu l, 1.27, and 6.98%, respectively, under the following experimental conditions: [Q(+)](T) = 2.30 x 10(-2) mol dm(-3), [PFOA(-)](T) = 5.75 x 10(-3) mol dm(-3), and 25 degrees C, This liquid phase was stable to physical changes such as Qi total concentration and temperature, compared with three other types of Q(+) ([4 . 4 . 4 . 4], [3 . 3 . 3 . 7], and [2 . 2 . 6 . 6]), which formed similar liquid-separated phases. (C) 1997 Academic Press
Doi 10.1006/jcis.1996.4543
Pmid 9056352
Wosid WOS:A1997WD07600033
Is Certified Translation No
Dupe Override No
Is Public Yes
Language Text English
Keyword form effect of quaternary ammonium ion; perfluorooctanoic acid; ion-pair association; phase separation phenomenon