Determination of chelating ability of antioxidants to Pb(II) using X-ray photoelectron (XPS) and UV-Vis spectroscopy

Chusuei, C; Chen, W

HERO ID

461153

Reference Type

Journal Article

Subtype

Abstract

Year

2008

Language

English

HERO ID 461153
Material Type Abstract
In Press No
Year 2008
Title Determination of chelating ability of antioxidants to Pb(II) using X-ray photoelectron (XPS) and UV-Vis spectroscopy
Authors Chusuei, C; Chen, W
Journal Free Radical Biology and Medicine
Volume 45
Issue Suppl.
Page Numbers S80-S80
Abstract Abstract: Previous research about the treatment of lead poisoning using an array of antioxidants, such as EDTA, penicillamine (Pen), selenocysteine (Sel), succimer, N-acetylcysteine (NAC) and N-acetylcysteine amide (NACA) showed differences in chelating abilities and levels of oxidative stress reduction. Chelation effects of these antioxidants to Pb(Ⅱ) were studied in vitro. Experiments were conducted at 0°C to 10°C, pH= 7.4 and with a 0.09% NaCl solution as the background electrolyte. UV-vis spectroscopy was used to determine the stoichiometry of the metal-to-ligand complexation within the antioxidant-Pb chelation. X-ray photoelectron spectrometer (XPS) was adopted as a direct and quick way to predict the effectiveness of antioxidants. NACA was found to be the most effective antioxidant for chelating Pb(Ⅱ) in the series. in addition, XPS confirmed that NACA reacted with Pb more easily by forming precipitates, as compared to the other antioxidants studied. These findings also demonstrate that XPS is a promising method for efficient, rapid evaluation of antioxidant Pb binding in vitro.
Wosid WOS:000260867900224
Url http://www.sciencedirect.com/science/article/pii/S0891584908006254
Is Certified Translation No
Dupe Override No
Conference Location Indianapolis, IN
Conference Name Society for Free Radical Biology and Medicine 15th Annual Meeting
Conference Date November 19-23, 2008
Is Public Yes
Language Text English
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