Synthesis of novel macrolactam and macroketone analogues of migrastatin from D-glucal and comparison with macrolactone and acyclic analogues: A dorrigocin A congener is a potent inhibitor of gastric cancer cell migration

Anquetin, G; Horgan, G; Rawe, S; Murray, D; Madden, A; Macmathuna, P; Doran, P; Murphy, PV

HERO ID

4947771

Reference Type

Journal Article

Year

2008

HERO ID 4947771
In Press No
Year 2008
Title Synthesis of novel macrolactam and macroketone analogues of migrastatin from D-glucal and comparison with macrolactone and acyclic analogues: A dorrigocin A congener is a potent inhibitor of gastric cancer cell migration
Authors Anquetin, G; Horgan, G; Rawe, S; Murray, D; Madden, A; Macmathuna, P; Doran, P; Murphy, PV
Journal European Journal of Organic Chemistry
Issue 11
Page Numbers 1953-1958
Abstract Novel macrolactam and macroketone analogues of the migrastatin macrolide core have been synthesised from tri-O-acetyl-D-glucal in order to facilitate structure-activity studies. The Horner olefination, followed by ring-closing metathesis were key steps in the synthesis of the macroketone. The ability of the macroketone and macrolactam derivatives to inhibit the migration of gastric tumour cells as determined using a transwell migration assay were compared with macrolactone analogues and dorrigocin A analogues. One dorrigocin A congener was the most potent inhibitor of gastric cancer cell migration. ((C) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2008).
Doi 10.1002/ejoc.200701192
Wosid WOS:000255144100013
Is Certified Translation No
Dupe Override No
Is Public Yes
Keyword carbohydrates; tumour cell migration inhibitor; cancer; Horner olefination; migrastatin; dorrigocin A natural products