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HERO ID
1589592
Reference Type
Journal Article
Title
Synthesis, thermal stability, and photocatalytic activity of nanocrystalline titanium carbide
Author(s)
Chen, Y; Zhang, H; Ma, D; Ma, J; Ye, H; Qian, G; Ye, Yi
Year
2011
Is Peer Reviewed?
1
Journal
Materials Research Bulletin
ISSN:
0025-5408
Volume
46
Issue
11
Page Numbers
1800-1803
DOI
10.1016/j.materresbull.2011.07.042
Web of Science Id
WOS:000296038700009
Abstract
Titanium carbide (TiC) was prepared via one simple route by the reaction of metallic magnesium powders with titanium dioxide (TiO(2)) and potassium acetate (CH(3)COOK) in an autoclave at 600 degrees C and 8 h. Phase structure and morphology were characterized by X-ray powder diffraction (XRD) and Scanning electron microscopy (SEM). The results indicated that the product was cubic TiC, which consisted of particles with an average size of about 100 nm in diameter. The product was also studied by the thermogravimetric analysis (TGA) and its photocatalysis. It had good thermal stability and oxidation resistance below 350 degrees C in air. In addition, we discovered that the cubic TiC powders exhibited photocatalytic activity in degradation of Rhodamine-B (RhB) under 500W mercury lamp light irradiation. (C) 2011 Elsevier Ltd. All rights reserved.
Keywords
Carbides; Chemical synthesis; Thermogravimetric analysis; X-ray diffraction; Catalytic properties
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