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HERO ID
1665545
Reference Type
Journal Article
Title
Surface characterization of LaCoO3 synthesized using citric acid
Author(s)
Taguchi, H; Yamada, S; Nagao, M; Ichikawa, Y; Tabata, K
Year
2002
Is Peer Reviewed?
1
Journal
Materials Research Bulletin
ISSN:
0025-5408
Volume
37
Issue
1
Page Numbers
69-76
Web of Science Id
WOS:000174787600007
URL
https://linkinghub.elsevier.com/retrieve/pii/S0025540801007991
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Abstract
In preparation for synthesizing LaCoO3, gel was prepared by adding citric acid to the aqueous solution of La(NO3)(3).6H(2)O and Co(NO3)(2).6H(2)O. The infrared spectrum indicates that the gel prepared with 0.007 mol of citric acid is the mixture of LaCo(C6H5O7)(NO3)(3), lanthanum nitrate, and cobalt nitrate, while the gel prepared with 0.011 mol of citric acid is LaCo(C6H5O7)(2). Perovskite-type LaCoO3 was obtained by firing the gel above 600degreesC. The LaCoO3 surface was characterized by X-ray photoelectron spectroscopy and with respect to the catalytic activity of CO oxidation. (C) 2002 Elsevier Science Ltd. All rights reserved.
Keywords
oxides; chemical synthesis; photoelectron spectroscopy; catalytic properties
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Nitrate/Nitrite
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