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HERO ID
1746089
Reference Type
Journal Article
Title
Solid-state synthesis of Sr- and Co-doped LaMnO3 perovskites
Author(s)
Ma, WH; Xie, G; Chen, SR; Cui, H
Year
2001
Is Peer Reviewed?
1
Journal
Transactions of Nonferrous Metals Society of China
ISSN:
1003-6326
Volume
11
Issue
6
Page Numbers
904-907
Web of Science Id
WOS:000172554300023
Abstract
The synthesis process for La1-xSrxMn1-yCoyO3-delta (x = 0.2, 0.3; y = 0.2, 0.8, designated as LSMC below) perovskite oxides prepared by solid state reaction was investigated using DSC/TG, XRD, EPMA and particle size analysis methods. It was found that LSMCs were all of single phase and the synthesis process might be divided into three stages: the decomposition of reactants, the formation of LaMn(Co)O-3-based oxides, and the formation of LSMC solid solution. Typical average and the peak value of particle size, and the specific surface area are 14.65 mum, 16.4 mum and 1.38 m(2)/mL, respectively, for mixed reactants and are 23.81 mum, 32.11 mum and 0.5 m(2)/mL, respectively, for powder synthesized at 1200 degreesC for 8 h in air.
Keywords
solid-state reaction synthesis; La1-xSrxMn1-yCoyO3-delta; perovskite; intermediate temperature SOFCs
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