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HERO ID
2651730
Reference Type
Journal Article
Title
Synthesis and properties of lead nanoparticles
Author(s)
Akimov, DV; Andrienko, OS; Egorov, NB; Zherin, II; Usov, VF
Year
2012
Is Peer Reviewed?
1
Journal
Russian Chemical Bulletin
ISSN:
1066-5285
EISSN:
1573-9171
Volume
61
Issue
2
Page Numbers
225-229
DOI
10.1007/s11172-012-0032-7
Web of Science Id
WOS:000312068000001
Abstract
Lead nanoparticles were synthesized by the thermal decomposition of lead stearate in octanol. The nanoparticles were characterized by X-ray powder diffraction, thermal analysis, IR spectroscopy, and electron microscopy. The lead particle size can be controlled by both varying the concentration of lead stearate in octanol and changing the thermolysis time. Lead nanoparticles have an organic coat composed of decomposition products of lead stearate. This coat prevents the particles from oxidation in air and favors their dissolution in organic solvents.
Keywords
lead; nanoparticles; synthesis; thermolysis; lead stearate
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