Determination of organotin compounds in water samples by solid phase microextraction (SPME) and GC./POISONING | Health & Environmental Research Online (HERO)

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Citation
Tags

HERO ID

2747506

Reference Type

Journal Article

Title

Determination of organotin compounds in water samples by solid phase microextraction (SPME) and GC./POISONING

Author(s)

Guidotti, M; Vitali, M

Year

1997

Is Peer Reviewed?

Yes

Journal

Annali di Chimica
ISSN: 0003-4592
EISSN: 1612-8877

Report Number

BIOSIS/97/26884

Volume

Issue

7-8

Page Numbers

7-8

Language

English

Abstract

BIOSIS COPYRIGHT: BIOL ABS. A method for the determination of organotin compounds in water by Solid Phase Microextraction (SPME) has been developed. The compounds are derivatizated with sodium tetraethylborate (STEB), extracted by a SPME fiber covered with a 100 pm polydimethylsiloxane coating and desorbed into the splitless injector of a gas chromatograph (GC) coupled with a mass selective detector (MS). Sub-ppb detection limits have been obtained and calibration curves were linear in the range investigated (1-50 ppb). Analyses of spiked river water prove the suitability of the method.