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HERO ID
2815809
Reference Type
Journal Article
Title
Stability of isoniazid in aqueous solutions containing sucrose or sorbitol
Author(s)
Hald, JG
Year
1969
Is Peer Reviewed?
Yes
Journal
Dansk Tidsskrift for Farmaci
ISSN:
0011-6513
Report Number
IPA/71/29100
Volume
Tidsskr
Issue
REF 2
Page Numbers
156-159
Language
English
Abstract
IPA COPYRIGHT: ASHP In the present paper it is shown that when stored, isoniazid in aqueous solutions of sucrose is probably decomposed by oxidation as well as by condensation. It is likely that the condensation is due to hydrolysis of sucrose to glucose and fructose, followed by formation of the corresponding isonicotinoyl hydrazones. The oxidation has been followed by bromometric titration. The untransformed isoniazid was condensed with benzaldehyde, extracted with chloroform as the benzaldehyde isonicotinoyl hydrazone and quantitatively determined by perchloric acid titration. Addition of sodium citrate reduces the rate of hydrolysis of the sucrose and consequently increases the stability. In aqueous solutions of sorbitol only oxidative decomposition affects the stability of isoniazid.
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