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HERO ID
337100
Reference Type
Book/Book Chapter
Title
Thermal analysis, effect of dopants, spectral characterisation and growth aspects of KAP crystals
Author(s)
Vasudevan, G; Anbusrinivasan, P; Madhurambal, G; Mojumdar, SC
Year
2009
Publisher
Springer, Dordrecht,
Location
N/A
Volume
96
Page Numbers
99-102
Language
English
DOI
10.1007/s10973-008-9880-7
Web of Science Id
WOS:000264133900018
Abstract
Potassium acid phthalate (KAP) which is also known as potassium hydrogen phthalate (KC[sup]8[/sup]H[sup]5[/sup]O[sup]4[/sup]), a semi-organic compound was grown from its aqueous solution only by slow evaporation method at room temperature. The effect of metallic salts HgCl[sup]2[/sup] and PbCl[sup]2[/sup] as dopants in the growth aspects, thermal properties and SHG efficiency of KAP were determined using UV-VIS, FTIR spectral studies, thermal (TG and DTA) analysis and NLO test. There is only one significant mass loss step on TG curve of pure and doped KAP crystal. DTA curve exhibit a higher peak temperature in case of doped KAP crystal compared to those of pure KAP crystals. (English)
Keywords
effect of dopants; HgCl2; KAP; PbCl2 spectral characterization; SHG efficiency; thermal analysis; Transformation Fourier; Spectrométrie IR; Spectrométrie UV visible; Analyse thermique différentielle; Thermogravimétrie; Plomb II Chlorure; Mercure II Chlorure; Optique non linéaire; Carboxylate; Sel organique; Potassium Composé; Génération harmonique 2; Cristal; Matériau dopé; Analyse thermique; 4270N; FT IR; Potassium phtalate; Fourier transformation; Infrared spectroscopy; Ultraviolet visible spectrometry; Differential thermal analysis; Thermogravimetry; Lead II Chlorides; Mercury II Chlorides; Nonlinear optics; Carboxylates; Organic salt; Potassium Compounds; Second harmonic generation; Crystals; Doped materials; EspectrometrÃa UV visible; Plomo II Cloruro; Mercurio II Cloruro; Sal orgánica; Compuesto
Edition
1
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