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HERO ID
3835795
Reference Type
Journal Article
Title
IONIC LIQUID [NMP]+HSO4-: AN EFFICIENT AND RECYCLABLE CATALYST FOR THE SYNTHESIS OF 1-AMIDOALKYL-2-NAPHTHOLS AND 1-CARBAMATOALKYL-2-NAPHTHOLS UNDER SOLVENT-FREE CONDITIONS
Author(s)
Deshmukh, KM; Qureshi, ZS; Patil, YP; Bhanage, BM
Year
2012
Is Peer Reviewed?
1
Journal
Synthetic Communications
ISSN:
0039-7911
Volume
42
Issue
1
Page Numbers
93-101
Language
English
DOI
10.1080/00397911.2010.522293
Web of Science Id
WOS:000297977000011
Abstract
A simple and efficient protocol for the one-pot synthesis of 1-amidoalkyl-2-naphthols and novel 1-carbamatoalkyl-2-naphthols has been described under solvent-free conditions, using N-methyl-2-pyrrolidone hydrogen sulfate (NMP+HSO4-) as a reusable Bronsted acidic ionic liquid. This methodology has several advantages such as use of a halogen-free ionic liquid NMP+HSO4-, excellent yields, short reaction time, easy workup procedure, and reusable catalyst.
Keywords
Aldehyde; amides; ionic liquids; multicomponent reaction; solvent free
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