Application of voltammetric methods for the analysis of lead and other trace metals in lepidolite rock sample | Health & Environmental Research Online (HERO)

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Citation
Tags

HERO ID

501805

Reference Type

Journal Article

Title

Application of voltammetric methods for the analysis of lead and other trace metals in lepidolite rock sample

Author(s)

Mishra, A; Pitre, KS

Year

2005

Is Peer Reviewed?

Yes

Journal

Journal of the Indian Chemical Society
ISSN: 0019-4522

Volume

Issue

Page Numbers

265-268

Language

English

Abstract

Convenient, simple, rapid and accurate voltammetric methods viz. DCP, DPP and DPASV have been used for the simultaneous determination of lead and other trace metals in lepidolite rock sample. The analysis has been performed using 0.1 M ammonium tartrate/0-1 M ammonium chloride/0-1 M lithium chloride as supporting electrolytes with 0.01% gelatin as maximum suppressor, respectively. The results show the presence of Pb-II (14.97), Zn-II (4.37), Fe-II (4.73), Cr-VI (3.36) and Co-III (7.42) mg g(-1) of the sample. The quantitative analysis of metal ions was carried out by external spiking method. Statistical treatment of the observed voltammetric data revealed high accuracy and good precision of determination. The observed voltammetric results are comparable with those obtained using atomic absorption spectroscopic (AAS) method.

Keywords

behavior