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HERO ID
604891
Reference Type
Journal Article
Title
A Green, Guided-Inquiry Based Electrophilic Aromatic Substitution for the Organic Chemistry Laboratory
Author(s)
Eby, E; Deal, ST
Year
2008
Is Peer Reviewed?
Yes
Journal
Journal of Chemical Education
ISSN:
0021-9584
Volume
85
Issue
10
Page Numbers
1426-1428
Abstract
The article focuses on electrophilic aromatic substitution (EAS) laboratory that can reduce the hazardous wastes generated in organic chemistry laboratories. EAS laboratory aims to secure the safety of the students and reduce the costs associated with wastes disposal, and it carries out a multistep procedure using aniline, acetic anhydride, and mixture of nitric and sulfuric acids to produce p-nitroaniline. An analgesic called Salicylamide is used as starting material for EAS because the directing effects of the substituents on the aromatic ring complements each other. The iodination of salicylamide is successfully adapted to generate iodine electrophile. Other details of EAS laboratory is also discussed.
Keywords
NITROAROMATIC compounds; CHEMICAL processes; SUBSTITUTION reactions; ANALGESICS; NITROANILINE; NITRIC acid; SULFURIC acid; ELECTROPHILES
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