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HERO ID
6360040
Reference Type
Journal Article
Title
Preparation of colloidal microporous carbon spheres from furfuryl alcohol
Author(s)
Yao, J; Wang, H; Liu, J; Chan, KY; Zhang, L; Xu, N
Year
2005
Is Peer Reviewed?
Yes
Journal
Carbon
ISSN:
0008-6223
EISSN:
1873-3891
Publisher
Elsevier
Volume
43
Issue
8
Page Numbers
1709-1715
DOI
10.1016/j.carbon.2005.02.014
Web of Science Id
WOS:000229986400014
URL
http://www.sciencedirect.com/science/article/pii/S000862230500117X
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Abstract
Colloidal microporous carbon (MC) spheres with an average size of 260nm1.5µm were prepared by carbonization of nonstick poly(furfuryl alcohol) (PFA) spheres, which were synthesized by a two-step polymerization of furfuryl alcohol (FA) involving slow polymerization (1st step) and sphere formation (2nd step). The high dispersibility of the MC spheres was simultaneously realized by removing surface functional groups of the PFA spheres with the evaporation-induced concentrated sulfuric acid (2nd step). By varying the temperature of slow polymerization, the spheres with different sizes could be simply synthesized. The studies also showed that surfactant and sulfuric acid treatment played an important role in the synthesis of colloidal PFA (MC) spheres.
Keywords
Porous carbon; Carbonization; Particle size
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