Health & Environmental Research Online (HERO)


Print Feedback Export to File
6671122 
Journal Article 
Preparation of metal organic frameworks MIL-101 (Cr) with acetic acid as mineralizer 
Zhang, LJ; Qli, F; Ren, JX; Ma, LB; Li, MQ; , 
2018 
IOP PUBLISHING LTD 
BRISTOL 
Pure metal organic frameworks MIL-101(Cr) was directly prepared without any purification treatment using acetic acid as mineralizer. The physical structure and morphology of the material were studied by means of power X-ray diffraction(XRD), thermogravimetric(TG), scanning electron microscope(SEM) and N-2 adsorption-desorption and compared with conventional MIL-101(Cr) which synthesized with hydrofluoric acid as mineralizer. The results demonstrate that the specific surface area and pore volume of the MIL-101( Cr) synthesized with acetic acid as mineralizer are superior to hydrofluoric acid as mineralizer. The MIL-101(Cr) sample synthesized with acetic acid as mineralizer is stable above 450 degrees C, higher than the MIL-101(Cr) synthesized with hydrofluoric acid as mineralizer. 
1st International Conference on Environment Prevention and Pollution Control Technology (EPPCT) 
Tokyo, JAPAN