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HERO ID
6679149
Reference Type
Journal Article
Title
Determination of manganese and chromium in foods by atomic absorption spectrometry after wet digestion
Author(s)
Tinggi, U; Reilly, C; Petterson, C; ,
Year
1997
Is Peer Reviewed?
Yes
Journal
Food Chemistry
ISSN:
0308-8146
EISSN:
1873-7072
Publisher
ELSEVIER SCI LTD
Location
OXFORD
Volume
60
Issue
1
Page Numbers
123-128
DOI
10.1016/S0308-8146(96)00328-7
Web of Science Id
WOS:A1997XA37400019
Abstract
Wet digestion procedures using acid mixtures of HNO3/H2SO4/HClO4 and HNO3/H2SO4 were investigated for their effectiveness for decomposition of food samples prior to determination of manganese (Mn) and chromium (Cr) by flame and Zeeman graphite furnace atomic absorption spectrophotometry. The addition of hydrofluoric acid (HF) to the mixture of HNO3/H2SO4 was also investigated for determination of Cr. All the acid mixtures rested were found to be satisfactory, but, for reasons of safety, HNO3/H2SO4 was the method of choice. No apparent matrix interferences or losses of analytes were encountered with the method used. Analysis of selected food samples found relatively high levels of Mn and Cr in most cereal products. Meats, dairy products (except for Cr in cheese), vegetables and fruits contained relatively low levels of both elements. (C) 1997 Elsevier Science Ltd.
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