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Citation
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HERO ID
6881212
Reference Type
Journal Article
Title
3 ',6 '-Bis(diethylamino)-3H-spiro[2-benzothiophene-1,9 '-xanthene]-3-thione
Author(s)
Su, BY; Zhan, XinQi; Guo, JNan; Zhou, YueF; Zheng, H; ,
Year
2008
Journal
Acta Crystallographica Section E-Crystallographic Communications
ISSN:
2056-9890
Publisher
INT UNION CRYSTALLOGRAPHY
Location
CHESTER
Page Numbers
O2068-U1468
PMID
21580934
DOI
10.1107/S1600536808031218
Web of Science Id
WOS:000260607800126
Abstract
The title compound, C28H30N2OS2, was obtained by thionation of 3 ',6 '-bis(diethylamino)-3H-spiro[isobenzofuran-1,9 '-xanthene]-3-one with 2,4-bis(p-methoxyphenyl)-1,3-dithiadiphosphetane disulfide (Lawesson's reagent). The planes of the two benzene rings of the xanthene system are inclined at a dihedral angle of 17.4 (1)degrees, and the plane of the dithiophthalide group and the planes through the two benzene rings of the xanthene system make dihedral angles of 80.2 (1) and 82.8 (1)degrees, respectively.
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