Synthesis of benzoylformic acid | Health & Environmental Research Online (HERO)

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Citation
Tags

HERO ID

6909242

Reference Type

Journal Article

Title

Synthesis of benzoylformic acid

Author(s)

Li, G; Jiang, Y; Huang, KeL; Liu, Z; Ding, P; ,

Year

2008

Is Peer Reviewed?

Yes

Journal

Journal of the Indian Chemical Society
ISSN: 0019-4522

Publisher

SCIENTIFIC PUBL-INDIA

Location

JODHPUR

Volume

Issue

Page Numbers

552-554

Language

English

Web of Science Id

WOS:000256937300014

URL

https://www.scopus.com/inward/record.uri?eid=2-s2.0-46349092689&partnerID=40&md5=387f25f864ff04b9ba2d55ca7099dc44
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Abstract

A new route for preparing benzoylformic acid (phenylglyoxylic acid) was studied by benzene as the starting material after Friedel-Crafts reaction with acetic anhydride, oximation by isopropyl nitrite, then hydrolysis by hydrochloric acid and sodium nitrite. Calculated on the basis of acetophenone, the final yield is 57.5%. The suitable. experimental conditions were also discussed.