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HERO ID
7856706
Reference Type
Journal Article
Title
An abnormal reaction of N-(2,4-dinitrophenyl)-L-proline with thionyl chloride
Author(s)
Xu, ZB; Guo, ZR
Year
2003
Is Peer Reviewed?
1
Journal
Chinese Chemical Letters
ISSN:
1001-8417
EISSN:
1878-5964
Volume
14
Issue
2
Page Numbers
133-134
Language
English
Web of Science Id
WOS:000181228600008
Abstract
N- (2,4-Dinitrophenyl)-4-amino-n-butyl aldehyde 3 was obtained with high yield oF 80% when N- (2,4-dinitrophenyl)-L-proline 1 reacted with SOCl2 at room temperature. However, the anticipated product N- (2,4-dinitrophenyl)-tetrahydropyrrolyl-2-(4-methylthiophenyl) ketone 2 did not be produced. The mechanism was discussed in this article.
Keywords
L-proline; 1-fluoro-2,4-dinitrobenzene(FDNB); N-(2,4-dinitrophenyl)-4-amino-n-butyl aldehyde
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