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8095069 
Journal Article 
Synthesis and crystal structure of {4-[2-(9Hexyl-9H-carbazol-3-yl)vinyl] phenyl} Dimethylamine 
Wang, HL; Xu, WY; Wang, DL; Zhang, B; Wu, H 
2007 
Yes 
Chinese Journal of Structural Chemistry
ISSN: 0254-5861 
26 
6 
691-694 
English 
The title compound {4-[2-(9-hexyl-9hexyl-carbazol-3-yl)vinyl]phenyl} dimethylamine has been synthesized by the well known Wittig reaction, and its crystal structure was determined by single-crystal X-ray diffraction analysis. It crystallizes in monoclinic, space group P21/c with a = 47.87(2), b = 10.222(4), c = 9.612(4) Aring;, β = 92.401(9)°, V= 4699(3) Å3, Z = 8, C28H32N2, M r = 396.56, Dc = 1.121 g/cm3, F(000) = 1712 and μ/(Moka) = 0.065 mm 1 .The final R and wR are 0.0793 and 0.1983, respectively for 3524 observed reflections with I> 2σ(I). In the title compound, the bond lengths are normal, and the crystal is stabilized by Van der Waals' forces. 
Crystal structure; N-hexyl-3-formylcarbazole; Wittig reaction