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HERO ID
8222307
Reference Type
Journal Article
Title
Dibromo isocyanuric acid as an ionic brominating agent, II: Perbrominations
Author(s)
Gottardi, W
Year
1969
Is Peer Reviewed?
1
Journal
Monatshefte fur Chemie / Chemical Monthly
ISSN:
0026-9247
EISSN:
1434-4475
Volume
100
Issue
1
Page Numbers
42-50
Language
German
DOI
10.1007/BF00938235
Abstract
Dibromoisocyanuric acid (DBI) in concentrated sulfuric acid, oleum or fluorosulfonic acid is used for one step perbrominations of aromatic compounds with deactivating substituents. The reactions are carried out at room temperature in extremly short reaction times (e.g. 1 min. for the perbromination of nitrobenzene in oleum) and-in part-good yields (near 90%). Comparison with other brominating agents of the N-Br type show the superiority of DBI. Tetrabromo-o-dinitrobenzene and dekabromo-diphenylketone were prepared for the first time. © 1969 Springer-Verlag.
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