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HERO ID
8222646
Reference Type
Journal Article
Title
Synthesis and spectroscopic studies of some metal complexes of (4-nitrobenzoyl) carbarmothioyl) histidine (NCH)
Author(s)
Gazi, A; Sarhan, BM
Year
2018
Volume
10
Issue
8
Page Numbers
33-41
Language
English
Abstract
(4-nitrobenzoyl) carbamothioyl) histidin (NCH) a new ligand was synthesized by reaction of Histidine with (4-Nitrobenzoyl isothiocyanate) by using acetone as a solvent. The prepared ligand (NCH) has been characterized by elemental analysis (CHNS), infrared (FT-IR), electronic spectral (Ultraviolet visible) and ( 1 H, 13C -Nuclear Magnetic Resonance) spectra. Some Divalent metal ion complexes of (NCH) were prepared and spectroscopic studies by Fourier transform infrared (FTIR), electronic spectral (UV-Vis), molar conductance, magnetic susceptibility and atomic absorption. The results measured showed the formula of six prepared complexes were [M (NCH) 2] (M +2 =Manganese, Cobalt, Nickel, Zinc, Cadmium and Mercury), from the obtained data tetrahedral structure suggested for all complexes, except Copper complex has a square planer geometry. ©2009-2018, JGPT. All Rights Reserved
Keywords
4-Nitrobenzoyl isothiocyanate; Histidin; Metal Ion complexes
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