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HERO ID
8313642
Reference Type
Journal Article
Title
A Crystalline Organo-Iron Pigment from a Rust Fungus (Ustilago sphaerogena)
Author(s)
Neilands, JB
Year
1952
Is Peer Reviewed?
Yes
Journal
Journal of the American Chemical Society
ISSN:
0002-7863
EISSN:
1520-5126
Volume
74
Issue
19
Page Numbers
4846-4847
Language
English
DOI
10.1021/ja01139a033
Abstract
A crystalline organo-iron pigment has been isolated from the cells of the rust fungus Ustilago sphaerogena. The organism was cultured by large-scale fermentation and the pigment extracted from the cells with dilute alkali. Ammonium sulfate was used to deproteinize the extract, the pigment was taken into benzyl alcohol and crystallized from methanol. The recrystallized material was homogeneous on chromatography and specific extinction coefficient tests. The presence of iron was proven by emission spectrography and analyses. In aqueous solutions, þH 4 to 10, there is a broad absorption band with a maximum at 425 mμ. A negative hemochrome test, in addition to other evidence, shows the substance does not have the nature of a heme compound. It is proposed to name the substance âferrichromeâ. © 1952, American Chemical Society. All rights reserved.
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