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HERO ID
8521771
Reference Type
Journal Article
Title
EPR spectroscopic characterization of local nanoscopic heterogeneities during the thermal collapse of thermoresponsive dendronized polymers
Author(s)
Junk, MJN; Li, W; Schlã¼Ter, AD; Wegner, G; Spiess, HW; Zhang, A; Hinderberger, D
Year
2010
Is Peer Reviewed?
Yes
Journal
Angewandte Chemie (International Edition)
ISSN:
1433-7851
EISSN:
1521-3773
Volume
49
Issue
33
Page Numbers
5683-5687
Language
English
DOI
10.1002/anie.201001469
Abstract
(Figure Presented) The collapse transition of thermoresponsive dendronized polymers was characterized on a molecular scale by CW EPR spectroscopy. Aggregation of the polymer is triggered by dynamic structural inhomogeneities of a few nanometers, and the dehydration of the polymer chains proceeds, despite the sharp phase transition, over a temperature interval of at least 30°C (see picture). © 2010 Wiley-VCH Verlag GmbH & Co. KCaA, Weinheim.
Keywords
EPR spectroscopy; Nanostructures; Non-equilibrium processes phase transitions; Polymers
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