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HERO ID
8707152
Reference Type
Journal Article
Title
The molecular structure of 1,3,5-trithiane from electron diffraction
Author(s)
Bencze, Z; Kucsman, A; Schultz, G; Hargittai, I
Year
1989
Is Peer Reviewed?
Yes
Journal
Acta Chemica Scandinavica
ISSN:
0904-213X
EISSN:
1902-3103
Volume
43
Page Numbers
953-956
Language
English
DOI
10.3891/acta.chem.scand.43-0953
Abstract
The molecular structure of 1,3,5-trithiane has been determined by gas-phase electron diffraction at 466 K nozzle temperature. The experimental data are consistent with the chair conformation of the molecule with C3v symmetry. The ring is considerably more puckered than that of cyclohexane. The following bond lengths (rg, bond angles and torsional angle were obtained: S-C 1.812 ± 0.004, C-H 1.114 ± 0.004 Å, C-S-C 99.1 ± 0.4, S-C-S 115.8±0.1, H-C-H 109.7 ± 1.2, S-C-S-C 65.2 ± 0.5°. 1989 Acta Chemica Scandinavica. All rights reserved.
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