Health & Environmental Research Online (HERO)


Print Feedback Export to File
1049829 
Journal Article 
NMR study on the structure and stability of 4-substituted aromatic iodosyl compounds 
Hiller, A; Patt, JT; Steinbach, J 
2006 
1 
Magnetic Resonance in Chemistry
ISSN: 0749-1581 
44 
10 
955-958 
English 
16900572 
WOS:000240999700009 
Two 4-substituted aromatic iodosyl compounds were investigated with regard to their solubility, stability and chromatographic behaviour. 1-Iodosyl-4-methoxy- and 1-iodosyl-4-nitro-benzene are soluble in methanol and provide acceptable 1H and 13C NMR spectra; however, gradual oxidation of the solvent was observed. LC-MS analyses suggest that unlike the parent substance, iodosylbenzene, which has a polymeric structure, both compounds rather exist in the monomeric form. 
NMR; H-1 NMR; C-13 NMR; aromatic iodosyl compounds; oxidation; HPLC-MS 
IRIS
• Methanol (Non-Cancer)
     Search 2012
          WOS