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HERO ID
2432720
Reference Type
Journal Article
Title
Synthesis and Crystal Structure of 1-(4-{[(E)-4-methoxy-2-hydroxybenzylidene]amino}phenyl)ethanoe Oxime
Author(s)
Dong, W; Wu, J; Wang, Li; Zhang, Y; Li, X; Li, Li
Year
2013
Is Peer Reviewed?
Yes
Journal
Asian Journal of Chemistry
ISSN:
0970-7077
EISSN:
0975-427X
Volume
25
Issue
11
Page Numbers
6156-6158
Language
English
DOI
10.14233/ajchem.2013.14296a
Web of Science Id
WOS:000325089600064
URL
https://www.scopus.com/inward/record.uri?eid=2-s2.0-84880016616&doi=10.14233%2fajchem.2013.14296a&partnerID=40&md5=ca43f309eeb82d88a5c1036a70eac806
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Abstract
The compound 1-(4-{[(E)-4-methoxy-2-hydroxybenzylidene]amino}phenyl)ethanoe oxime with the molecular formula C16H16N2O3, has been synthesized and characterized structurally. The two benzene rings in the molecule form a dihedral angle of 3.05(2)degrees. There is one strong intramolecular O-H center dot center dot center dot N hydrogen bond between the hydroxyl (O2-H2) groups and the Schiff base nitrogen (N2) atom, with the distance of d(N2-O2) = 2.593(4)angstrom. In the crystal structure, each molecule links other three molecules into an infinite 2D supramolecular structure by three pairs of intermolecular O1-H1 center dot center dot center dot N1, C1-H1A center dot center dot center dot O1 and C16-H16B center dot center dot center dot O3 hydrogen bonds.
Keywords
Mono-oxime compounds; Synthesis; Crystal structure
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