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2612405 
Journal Article 
Mechanochemical synthesis of vanadium nitride 
Roldan, MA; Lopez-Flores, V; Alcala, MD; Ortega, A; Real, C 
2010 
Yes 
Journal of the European Ceramic Society
ISSN: 0955-2219 
30 
10 
2099-2107 
WOS:000278651400014 
Vanadium nitride (VN) has been prepared by mechanosynthesis from vanadium metal under a pressurized nitrogen atmosphere in a short milling time. The characterization of the final product by X-ray diffraction, scanning electron microscopy, electron energy loss (EELS), and X-ray absorption spectroscopy (XAS) is presented. The final product, VN with 96% of purity, is obtained at room temperature with nanometric particle size and a very high microhardness after sintering. A relationship between microstructure and microhardness as well as a comparison between the VN obtained mechanical and thermal method is also presented. (c) 2010 Elsevier Ltd. All rights reserved. 
Mechanosynthesis; Vanadium nitride; EELS; XAS; Microhardness