Analysis of nitrophenols and other polar nitroaromatic compounds in ammunition wastewater by high-field proton nuclear magnetic resonance (1H-NMR) spectroscopy and chromatographic methods | Health & Environmental Research Online (HERO)

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Citation
Tags

HERO ID

629400

Reference Type

Journal Article

Title

Analysis of nitrophenols and other polar nitroaromatic compounds in ammunition wastewater by high-field proton nuclear magnetic resonance (1H-NMR) spectroscopy and chromatographic methods

Author(s)

Preiss, A; Lewin, U; Wennrich, L; Findeisen, M; Efer, J

Year

1997

Volume

357

Issue

Page Numbers

676-683

Language

English

Abstract

BIOSIS COPYRIGHT: BIOL ABS. It is shown that by using high-field proton nuclear magnetic resonance (1H-NMR) spectroscopy it is possible, without prior separation, to analyse nitrophenols and other acidic nitroaromatic compounds in the "pH 2 extract" of ammunition wastewater. The 1H-NMR chemical shifts data of a variety of reference compounds are presented. Two groundwater samples from the former ammunition plant in Elsnig (Saxony) were analysed by 1H-NMR and also by chromatographic methods (GC, HPLC). The results are compared and discussed./POISONING

Keywords

Biochemistry methods; Biochemistry; Biophysics methods; Poisoning; Animals; laboratory; Environmental pollutants poisoning; Occupational diseases; 5460-31-1; 4920-77-8; 2691-41-0; 2581-34-2; 2423-71-4; 2042-14-0; 700-38-9; 619-17-0; 610-30-0; 609-93-8; 586-11-8; 577-71-9; 573-56-8; 554-84-7; 552-16-9; 534-52-1; 528-45-0; 131-73-7; 129-66-8; 121-92-6; 121-82-4; 119-33-5; 100-02-7; 99-34-3; 88-89-1; 88-75-5; 66-56-8; 62-23-7; 51-28-5