Quantitative oxidation of some phenols using potassium dipertellurato cuprate (III) as oxidant at milligram scale | Health & Environmental Research Online (HERO)

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Citation
Tags

HERO ID

1344402

Reference Type

Journal Article

Title

Quantitative oxidation of some phenols using potassium dipertellurato cuprate (III) as oxidant at milligram scale

Author(s)

Chauhan, RPS; Siddiqui, MA; Mishra, G; Kumari, KK

Year

1998

Is Peer Reviewed?

Journal

Oxidation Communications
ISSN: 0209-4541

Volume

Issue

Page Numbers

211-215

Web of Science Id

WOS:000074881300009

Abstract

An accurate method has been described for the determination of phenols milligram level with the use of potassium dipertellurato cuprate(III) reagent as oxidant. The sample reacted with the excess of Cu(III) solution on a hot plate for reflux for about 15 min. When the reaction was over the content was cooled to room temperature. The unreacted Cu(III) reagent was estimated by the arsenite method. A blank was also run under identical conditions using all reagent except the sample. The precision and accuracy are within +/- 1%.