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HERO ID
1453699
Reference Type
Journal Article
Title
Solubility of N-chloro succinimide in different pure solvents in the temperature range from 278.15 K to 333.15 K
Author(s)
Zhu, J; Shen, Fei; Hu, YH; Jiang, Xinmin; Li, Dyun
Year
2012
Is Peer Reviewed?
1
Journal
Korean Journal of Chemical Engineering
ISSN:
0256-1115
EISSN:
1975-7220
Volume
29
Issue
10
Page Numbers
1413-1417
DOI
10.1007/s11814-012-0061-9
Web of Science Id
WOS:000309615700019
Abstract
Solubility data were measured for N-chloro succinimide in
pure n-butanol, ethyl acetate, acetone, isopropanol, tetrahydrofuran, acetonitrile and acetic
anhydride at the temperature range between 278.15 K and 333.15 K under atmospheric pressure by
gravimetric method. The solubility of N-chloro succinimide in those selected solvents increased
with increasing temperature. The solubility data were correlated with the modified Apelblat
equation and the van't Hoff equation to obtain the model parameters. The experimental results
could be useful for optimizing the process of purification of N-chloro succinimide in industry.
Isopropanol could be the excellent solvent in the crystallization of N-chloro succinimide.
Keywords
N-chloro Succinimide; Solubility; Measure; Correlation
Tags
IRIS
•
Methanol (Non-Cancer)
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