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5933145 
Journal Article 
One-step controlled electrodeposition of iron-based binary metal organic nanocomposite 
Zhang, B; Huang, Pin; Chen, J; Dang, X; Hu, Y; Ai, Y; Zheng, D; Chen, H 
2020 
Yes 
Applied Surface Science
ISSN: 0169-4332 
Elsevier B.V. 
AMSTERDAM 
504 
144504 
English 
WOS:000502040600146 
A cauliflower-shaped Fe/Fe-BTC nanocomposite was prepared by one-step controlled cathodic electrodeposition method. The obtained Fe-BTC nanoscale film was characterized by scanning electron microscopy (SEM), energy-dispersive spectrometer (EDS), X-ray photoelectron spectroscopy (XPS), Fourier transform infrared spectra (FT-IR), thermogravimetric analysis (TGA) and electrochemical measurements, indicating its morphology, structure and electrochemical activities varied with the applied cathodic potential. The electrodeposition process was investigated thoroughly and the electrosynthesis mechanism of the Fe/Fe-BTC nanocomposite was proposed. The Fe/Fe-BTC nanoscale film deposited at - 1.5 V exhibited the loosest morphology and best electrochemical activity, which showed the best application potential in electrocatalytic H2O2 reduction and adsorption of diethyl phthalate (DEP) and dibutyl phthalate (DBP). The iron-based binary metal organic materials were designable and could be applied in the field of electrocatalysis and extraction. 
Metal organic materials (MOMs); Fe/Fe-BTC nanocomposite; Electrodeposition; Electrocatalysis; Adsorption 
IRIS
• Diethyl phthalate (DEP)
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