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Citation
Tags
HERO ID
1988282
Reference Type
Journal Article
Title
LC-TOF/MS determination of phthalates in edible salts from food markets in Korea
Author(s)
Dirwono, W; Nam, Y; Park, H; Lee, KB
Year
2013
Is Peer Reviewed?
Yes
Journal
Food Additives and Contaminants: Part B: Surveillance
ISSN:
1939-3210
EISSN:
1939-3229
Volume
6
Issue
3
Page Numbers
203-208
Language
English
PMID
24779906
DOI
10.1080/19393210.2013.795194
Web of Science Id
WOS:000323634600010
Abstract
Residual quantities of 12 phthalates have been monitored in edible salts (raw salts, refined salts, refined salts with additives and baked salts) available in Korean food markets. Liquid-liquid extraction followed by liquid chromatography time-of-flight mass spectrometry (LC-TOF/MS) was used to analyse the samples. The method was validated and showed linear correlation (R-2>0.996) in the range 0.5-100ngg(-1) for all target analytes. Recoveries were 85.9-108.4%, except for diethyl phthalate (DEP). Relative standard deviations (RSDs) were 2.7-6.0% and the limits of detection (LODs) were 1.2-2.8ngg(-1). Although the contamination of phthalates in salt would be trivial in comparison to those of other main foods and below the reference dose of the Chronic Oral Exposure recommended by US-EPA, the availability of reference data could be valuable for food chemists and salt manufacturers.
Keywords
phthalate; edible salt; unrefined raw salt; baked salt; LC-TOF/MS
Tags
IRIS
•
Diethyl phthalate (DEP)
Database searches
Aug 2013 update
Web of Science
Jul 2014 update
Web of Science
Jan 2020 update
PubMed
Web of Science
Excluded: No Primary Data on Health Effects
Measurement methods
•
Phthalates – Targeted Search for Epidemiological Studies
Source – all searches
Pubmed
Excluded
Source – Dec 2014 Update (Private)
Pubmed
Source – Mar 2015 Update (Private)
Pubmed
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